Syllabus for Chemistry Laboratory I (CH252) 

 

Course Information

1) Lecture: Experiment: Credit = 0: 6h: 2

2) Except for the final presentation, all the experiemnt will be performed in person off line, unless there is a further notice.

    Location: Goong-Ni Laboratory Building(E6-5), room 704

3) Instructor: Class A-Prof. Sang Woo Han, B- Prof. Woo Youn Kim, C- Prof. Kiyoung Park

4) Time Table

Time

Mon

Wed

Fri

13:00 ~ 19:00

A

Prof.

한상우(Han, Sang Woo)

     

C

Prof.

박기영(Park, Kiyoung)

TA

 

   

TA

 

 

Objectives for the Course

1) Skills relating to learning chemistry: Making chemistry real by illustrating ideas and concepts, exposing theoretical ideas

    to empirical teaching and teaching new chemistry.

2) Practical skills: Handling equipment and chemicals, learning safe scientific practices, masteringspecific techniques, measuring

  accurately, and observing carefully.

3) Scientific skills: Learning the skills of observation and the skills of deduction and interpretation. Appreciation of the place

of the empirical as a source of evidence in inquiry. Learning how to devise experiments that offer insights into chemical phenomena.

4) General skills: Numerous useful skills to be developed such as team working, reporting, presenting, discussing, time management,

and problemsolving skills.

 

Course Requirement

    1) Preparation in advance for experimental work

       (a) Pre-laboratory reading preparation for successful experiment

       (b) "Pre-lab"quizzes are or pre-lab reports are required relating to the experimental details.

    2) Wearing of eye protection and lab clothing at all times while in the laboratory.

    3) Writing up and submission of lab reports. Includes the following (but see evaluation)

        (a) Observations and experimental detail

        (b) Detailed method of processing the experimental data(for Quantitative analytical experiment)

        (c) Calculations and Conclusions regarding the accuracy and the precision of experimental  

             results and errors and the inherent errors based on the measurements

 

Grading

 5 Experiments (75 pts) + Final Presentation (25 pts)

  A+: 95 >, A0:90 >, A0:80 >, B+:70 >, B0:60 >, B-:50 >, C+:40 >, F:< 40

 

 

Methods of Evaluation

The student will be evaluated based on his/her performance of the requirement listed below.

 

 Point distribution per One Experiment = 15 pts

 

          1) Pre- laboratory Interview  (0 points)

             (a) Before starting experiments, everyone has to answer for questions by TA.

             (b) The questions about theoretical background, procedure, and safety.

             (c) One has to pass the interview to initiate experiments.

            

          2) Attitude (5 points)

            (a) Lateness (-2 pts)

            (b) Lab Safety  (-3 pts)

            (c) Cleanliness (-2 pts)

            (d) Concentration  (-2 pts)           

 

           3) Post-Laboratory Reports (10 points)

             (a) Data & Results (6 pts)

               - Lab note (3 pts)

               - Quantitative results: Data & Calculation, Table & Graphs (3 pts)

             (b) Discussion  (4 pts)  

                -Assessing the results

                -Conclusions

 

                     Final Presentation (25 pts, 15 min per group)

                                 - Topic will be chosen randomly two weeks before the presentation.

 

 

Lab Report Submission

1) Online submission:www.turnitin.com

2) Create your accout. Enter Class ID and Password (provided by TA)

3) Enter your name in Korean (한글로 이름과 성 입력)

4) Post-ab report submission due: Midnight, 7 days after the current experiment

5) Submitting a post-lab report, it should include the corresponding pre-lab report.

6) Plagiarism results in zero for all reports involved (Determined by TAs and Professor).

7) Late submission of post lab reports (after 72 hours from the due date) is not allowed.

 

Examination Information

     No Exams.

 

Reference

       1) handbooks

            (a) CRC handbook of Chemistry and Physics (CRC press, Boca Raton, Florida)

            (b) Merck Index(Merck & Co., Rakway, New Jersey)

            (c) Lange's Handbook of Chemistry (MaGraw-Hill, New York)

 

Tentative Schedule and Topics

 

    (a) Schedule

Week

Date

(Mon, Wed, Fri)

13:00~19:00

Experiment #

Assignment of experimental group per Exp# for rotation

Exp1

Exp2

Exp3

Exp4

Exp5

1

8/28,  9/1

Exp0: Orientation

 

 

 

 

 

2

9/4,  9/8

[Exp1 ~ Exp5]

1

2

3

4

5

3

9/11,  9/15

[Exp1 ~ Exp5]

6

7

8

9

10

4

9/18,  9/22

[Exp1 ~ Exp5]

5

1

2

3

4

5/6

9/25,  10/6

[Exp1 ~ Exp5]

10

6

7

8

9

6/7

10/2, 10/13

[Exp1 ~ Exp5]

4

5

1

2

3

8

10/16~ 10/20

Mid-term Exam Period

 

 

 

 

 

9

10/23,  10/27

[Exp1 ~ Exp5]

9

10

6

7

8

10

10/30,  11/3

[Exp1 ~ Exp5]

3

4

5

1

2

11

11/6,  11/10

[Exp1 ~ Exp5]

8

9

10

6

7

12

11/13, 11/17

[Exp1 ~ Exp5]

2

3

4

5

1

13

11/20, 11/24

[Exp1 ~ Exp5]

7

8

9

10

6

14

11/27, 12/1

Make-up experiment & presentation preparation]

 

 

 

 

 

15

12/4, 12/6, 12/8

Final Presentations

 

 

 

 

 

16

12/11 ~ 12/15

Final Exam Period

 

 

 

 

 

Detailed information will be notified on KLMS.

 

  (b) Topics

 

Topics

 

Exp0. Introduction , Work Instructions, and Laboratory Safety

 

 

Exp1. Electrochemistry

김연우, 최수빈

[Exp1-1]&[Exp1-2]

Exp2. IR/ Raman/ SERS Spectroscopy and Selection Rules

김다빈, 윤초록

[Exp2-1] & [Exp2-2]

Exp3. Computational Chemistry and Quantum Tunneling

정재우, 김수민

[Exp3-1]&[Exp3-2]&[Exp3-3]

Exp4. Life Time of Fluorescence

민병기, 김진우

[Exp4-1]&[Exp4-2]

Exp5. Atomic Force Microscope

안호찬, 표의정

[Exp5]